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Salvia divinorum extraction log


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#1 reverend trips

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Posted 20 August 2006 - 04:40 PM

I've been meaning to do an extraction with some of my harvest from last years salvia grow and finally found the time to get started.
Here is a pic of the plants from last year:
mexi 069.jpg
The great thing about salvia is that if it is dry and kept out of light it doesn't degrade.
Here's The dried leaves before grinding:
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Here they are after the long painstaking task of grinding them in the coffee grinder. I can't seem to get my blender to do it very well, the leaves just sit above the blades.
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This extraction will be done with 400 grams of leaf and I'll make it into 40 grams of 10x extract. Some will be donated for the midsummer raffle here:)
I've extracted salvia a few times before and found that if you take the extra steps to make your extract clean, it will be far less harsh.
I have tried just doing a straight acetone extraction and found that the extract was to so full of tannins that it was too gooey to even smoke.
The active ingredient is not soluble in water, so you can leech some of the junk out by soaking it in cool water for a few minutes.
I use cheesescloth from the grocery store and double it up, and line it in a pot.
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The ground up leaf goes in the pot and close the cheesecloth around it and fill with cool distilled water. You'll need to find something to weigh it down with to keep it submerged.
Let it sit like that for 5 or 10 minutes.
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Now pull it out and ring as much water out of it as you can and put the wet leaf in a large baking pan.
Here is a pic of the nastiness in the water that would have ended up in the extract if you hadn't done this step:
DSC00595.JPG
Now you'll need to get that wet leaf perfectly dry again before you can go on.
Heat you stove up to 185 and through the baking pan full of the wet leaf in and stir it up every hour or so.
This will take most of the day if you have a large amount.
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When you are sure it is completely dry you can load your leaf in mason jars.
I fill them up half way to leave lots of room for the acetone.
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This is the part when the wife send you to the garage beacause whe puts up with lots, but acetone in the house she will not put up with.
Make sure whatever brand of acetone you use is clean, I haven't found any around here that evaporates clean from the hardware stores, but I have a friend that uses reagent grade acetone at his work and hooks me up.
You can always distill the hardware store stuff yourself.
Fill the mason jars up with acetone give it a stir.
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Put the lids on upside down so the seal doesn't desolve from the acetone and cover it up with something to keep light from destroying it.
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This will now soak for 24 hours, I'll go out and stir it up a couple of times.
This is as far as I've got with this, I'll finish up this log as I do it.

#2 eu_por_exemplo

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Posted 20 August 2006 - 04:43 PM

So great Man! :bow:

#3 reverend trips

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Posted 21 August 2006 - 07:28 PM

Thanks, eu por exemplo:)
Ok the jars have been soaking for a day now, so it's time for the next step.
I use a steel strainer because acetone can desolve plastic and we don't need any unwanted chemicals in the extract.
Put a large coffee filter in the strainer and put that over a glass jar of some kind to hold the liquid.
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Pour as much of the liquid out of the jars as you can without dumping you leaf out.
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Do this till all your jars are done.
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Now fill the jars with the leaf back up with fresh acetone, cover again and let the sit for another day.
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Now put a fan on the filtered liquid, and cover windows or do whatever you have to do to keep light away.
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This will continue tomorrow...

#4 reverend trips

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Posted 27 August 2006 - 02:15 PM

Ok I've evaporated the acetone off, and let it sit for a few days.
What can I say, I'm lazy:)
Here is what was left after evaporated:
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Scraped it all out and put it in a spice jar for further refinement.
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To clean it up more use naptha.
I'll fill the spice jar up with naptha and stir it up and let it sit in a cupboard and settle for a couple of hours away from light.
Salvinorin is not soluble in naptha but will soak up chlorophyll nicely.
When a couple of hours is up, I'll pour out the top 2/3rds of the jar carefully.
Fill the jar back up with clean naptha, stir and again back in the cupboard for a couple hours.
I've done this 4 times now and I'm starting to get it clean enough to see the salvinorin layer on the bottom of the spice jar.
DSC00634.JPG
I'll keep doing this untill the naptha doesn't take on a dark colour, could be 5 more times.
Thats it for now...

#5 Hippie3

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Posted 27 August 2006 - 02:24 PM

wow, how'd i miss this for a week ?
great write-up
maybe i missed it,
what will the end concentration be,
i.e. ?x

#6 reverend trips

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Posted 27 August 2006 - 02:27 PM

It's going to be 10x Hip... thats plenty strong enough for me:)

#7 reverend trips

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Posted 27 August 2006 - 02:35 PM

I'll send some in as soon as it's finished for the raffle.

#8 mycobri

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Posted 27 August 2006 - 02:54 PM

:kewl: have you ever used ethanol for extracting salvinorin?

#9 reverend trips

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Posted 27 August 2006 - 03:56 PM

have you ever used ethanol for extracting salvinorin?

I have not, I got a good source for good acetone, and it works great.
Have you?
Is there any advantages to using it?

#10 reverend trips

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Posted 01 September 2006 - 06:00 PM

I've cleaned it up as far as I'm going to, I could get it cleaner but it will be a smooth smoking extract the way it is.
Here's what it looks like:
DSC00653.JPG
The dark stuff is from the evaporating naptha, but it is pretty clean.
I got 40 grams of leaf set aside that I maticulously went through and tried to get as much of the spines of the leaves out of, because I hate filling a bowl that has those in there.
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I redesolved the extract in fresh acetone and mixed it all in with the leaves.
I needed to add extra to make sure the leaf was saturated.
DSC00655.JPG
I mixed it all up and I'm waiting for it to evaporate off, and I'll be done.
Took a week or so longer then it should, but like I said before, I'm lazy!

#11 mycobri

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Posted 01 September 2006 - 07:44 PM

I have not, I got a good source for good acetone, and it works great.
Have you?
Is there any advantages to using it?


i'm not sure of the advantages, but i just used 151 spyrtus to extract 14g of leaf, then soaked 2 grams of leaf in the evaporating liquid until it was dry. i guess it would be 7x, i have not tested it. the cool thing about the extraction is the color the alcohol turned - emerald green.

nice job Reverend!

#12 reverend trips

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Posted 01 September 2006 - 08:17 PM

Cool, let us know how it is.
I'll be testing this batch out sometime tomorrow...

#13 robman1

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Posted 02 September 2006 - 04:31 PM

http://imageevent.com/sphere

#14 Guest_cap_*

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Posted 23 September 2006 - 06:37 AM

millions of thanks for this thread, rev!
:dance: you make it look so easy :D
that reagent grade acetone would come in handy right now
im washing some cannabis shake today/nite
hope all is well rev_trips and m_bri
cheers fellas :rasta:

#15 reverend trips

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Posted 23 September 2006 - 06:49 AM

Hey Cap, you are most welcome.
I'm pretty rich with canna shake lately too, I'm a big fan of the butane when it comes to making oil.
All the best!

#16 Guest_cap_*

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Posted 23 September 2006 - 06:58 AM

i am worried ill fuck something up :D
buyin an tri-tube from okief.com when i can afford it tho :D
thanks for the feedback rev!



I'll be testing this batch out sometime tomorrow...
verdict? :teeth:

#17 explorerowid

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Posted 23 September 2006 - 12:03 PM

Nice thread reverend...I love all the pics
I have never tried 10x, but i have tried 20x .

It was an experience to say the least.
I am not sure I will ever try Sally D again.

I used it for the wrong reason and it sure fucked my head up.
Good luck with testign it out and be respectful when you do.

E.E.

#18 Hippie3

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Posted 10 October 2006 - 11:37 AM

I'll send some in as soon as it's finished for the raffle.



rec'd
:bow:

#19 reverend trips

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Posted 11 October 2006 - 05:28 PM

Feel free to burn some Hip:hippie:

#20 shadowechos

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Posted 17 October 2006 - 01:33 AM

any places in our area you could recommend for the ethanol?
pardon my ignorance, but do you know if any old liquor store have it?
shoot me a pm bud! we need to catch up anyway man! been way too long


Don't know where you live--but in some liquor storea they carry it it's called "Everclear" a very high proof food grade alcohol




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