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DMT HCl -- titration pictorial


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#1 synth

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Posted 25 July 2007 - 06:22 AM

for more info, see:
http://mycotopia.net...ts-uh-whoa.html

300mg of fairly pure dmt freebase placed in a tube:

http://mycotopia.net...achmentid=57080

http://mycotopia.net...achmentid=57081

5 mL dH2O added:

http://mycotopia.net...achmentid=57082

the tube was shaken up a bit. apparently water is denser than dmt.

http://mycotopia.net...achmentid=57083

with much shaking, the dmt coated the wall of the tube and appeared
hydrophobic.
concentrated HCl was added dropwise with a pasteur pipet. after the
addition of each small droplet, the tube was shaken a lot and was warmed with a flame.
the pH was checked a few times before the endpoint. it was slightly basic.
at the endpoint, all of the dmt dissolved from the wall of the tube, and
the solution was slightly acidic.

the amount of HCl used in the titration was not measured.

http://mycotopia.net...achmentid=57084

joy. 15 or so doses ready to go.

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#2 Guest_vinz_*

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Posted 25 July 2007 - 08:04 AM

amazing work synth!
how's the dosage done and measured?

#3 Seee

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Posted 25 July 2007 - 09:24 AM

I know you say the HCl was not measured
but can you guesstimate
how many drops?
or how many times it was heated and shaken while the HCl was being added?

#4 synth

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Posted 25 July 2007 - 09:32 AM

doses will be measured by volume.

the drop sizes varied. near the end, very small amounts were added at a time.
probably close to 10 additions were made.

guesstimation? perhaps around 5 eyedropper sized drops.

#5 Hippie3

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Posted 25 July 2007 - 09:59 AM

:kewl:

#6 prankster239

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Posted 25 July 2007 - 10:19 AM

Great :headbang: I love pictorials

#7 NEPHROSIS

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Posted 25 July 2007 - 12:35 PM

What does applying heat do?

#8 smacked12

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Posted 25 July 2007 - 03:07 PM

going the iv route, you're a braver man than i am!

i always picture a broken needle sticking out of my arm. or worse yet a little impurity riding around in my veins eventually causing my heart to explode.

#9 Caljet666

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Posted 25 July 2007 - 03:20 PM

LOL.

A little impurity should pose no hazard so long as it is water soluble. The amount of shit thats traveled swim's circulatory system in the day is nothing short of scary but he appears to have no ill effects from his wilder days.

An exam by the doctor told swim this, the doctor stating that it is amazing what the body can withstand being shot into its blood stream

Nice write up synth and good pics. Clear and concise. Swim is wondering. Has anyone ever tried IV harmala alkaloids? Could be wild.

#10 Doctor D

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Posted 25 July 2007 - 05:29 PM

Cool, synth! Keep us posted, please! I'm very interested to know if IV spice causes more consistent breaks through for a given dose.

#11 synth

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Posted 25 July 2007 - 06:42 PM

I'm very interested to know if IV spice causes more consistent breaks through for a given dose.


it does. it's pretty much a sure thing.

#12 Lefty

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Posted 28 July 2007 - 09:24 AM

My compliments on the pics. Why not just gas it?

#13 synth

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Posted 29 July 2007 - 01:12 AM

ty.

why gas it?
the dmt was already at the desired level of purity.
all that's left to do is salt it.
i guess a better way to do this would be to salt with excess HCl(aq),
let it all evaporate, add water, and run it through a disk/wheel filter.

speaking of which.. i wish usps would hurry up. i want my filters.

#14 Lefty

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Posted 29 July 2007 - 11:41 AM

Seems like an okay way to add a hydrochloride, gas that is. Use of certain solvents for certain applications may allow only what one is after to precipitate.
Nice one, certainly not questioning purity level by the looks of it. Sometimes it's just nice to watch them fall again and maybe gain that .07% or so.

#15 AndyLandy420

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Posted 05 November 2008 - 06:54 PM

Excess HCl to the vein seems like the definition of uncool to me. Here is a little something i made up, errr distorted from other teks i've read.

take your finished clean dry DMT freebase and weigh precisely how much you are going to salt. the numbers I go with are as follows, .247mg per kg freebase is what strassman calls a full dose, so weigh precisley 247mg of freebase and when it comes time to dilute it, do so with precisely 10ml of water, then 1ml (100units) of solution is equal to 100KG bodyweight, so if you weigh 50kg then .5ml (50units) is a full dose for you. back to salting, take your spice and put it a small vial, place this vial loaded with spice up right inside a larger glass jar. have a good pile of anhydrous CaCl (damp-rid) on the bottom of the larger vessal. let it sit for a few days to be absolutely sure the spice is dry, then dump a slosh of HCl onto the CaCl and seal the jar, the CaCl will absorb the water and drive the HCl into vapor, this vapor will salt the freebase DMT and leave no excess since the spice is 'dry' (without water) and HCl must be aq (dissolved in water) to stick around. the finished goo should be absolutely nuetral DMT HCl, ready to be dissolved, filtered, and injected.




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