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Whatcha's Easy MHRB STB Extraction, Step by Step Pictorial


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#1 whatchamacallit

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Posted 05 September 2009 - 02:02 PM

This pictorial has been made by SWIM and given to me with permission to post it. It has step by step pics, with added details for each caption, that should make a simple to follow tutorial, with every day items anyone can purchase locally, with the exception of perhaps the bark and lye.

The utensils are everyday items, and makeshift tools from beverage containers mostly. This tek includes the polar wash and epsom salt dry in great detail, so people may get their DMT smooth smoking and free of any residual lye.

The recrystallization will be added to this thread as soon as time permits, so please enjoy, and take precautions to be safe when handling lye and solvents, such as protective glasses and solvent gloves.

So here goes!

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First, 1 lb of lye is added slowly to each gallon jug, that has been filled about halfway with cold tap water. To do this safely, SWIM places the jugs into a bathtub or sink, and runs cold water to go about halfway up the jugs. He makes sure that the water outside doesn't exceed the height of the water inside the jugs, or they will float and won't sit right in the sink or tub.

He then takes a 2 liter bottle that has the bottom cut off, and is clean and dry and places it into the top of the gallon jug. He slowly pours the lye in, about 1/3 of the lb at a time, then gives them a vigorous shake. He releases the pressure as they heat rapidly, and recaps it, then places it into the cold bath.

He shakes it more, and it heats again. Each time the jug begins to get hot, he sets it back into the cold bath, to keep the jug from getting soft. When the jug no longer heats when shaken, he adds the next bit of lye, until all the lye has been added to the half gallon of water in the jug. Once it is all added, he again shakes the crap out of it. He continues shaking and setting into the cold bath, until when shaken the jug no longer heats.

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The jugs are removed from the cold bath. He takes his powdered MHRB as shown here and begins to weigh out 454 grams, or 1 lb of MHRB into a cup.

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The 2 liter funnel is placed into the jug, and the MHRB is poured into the funnel. To make it easier to get the MHRB powder into the jug, he takes a butter knife and agitates the bark in the 2 liter, poking it down into the hole, so the hole is not clogged.

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This pic shows after 1 lb of bark has been added to each 1 gallon jug, that is half filled with lye water.

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Both jugs are shaken vigorously, as shown above.

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The jugs are then topped off with a little bit more hot tap water, but allowing enough room for 400 mls of VM&P Naphtha, and room to shake and easily pour. By adding a bit more water at this stage, it allows the MHRB/lye/water to be a little thinner and not too sludgy.

These jugs are then left to sit in the heat bath for at least one hour, to allow any DMT freebase to be loosened from the tiny bark particles. The jugs are shaken periodically during the hour or so, and set back in the heat bath. Once the hour has passed, it's on to the next step..

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Now, 400 mls of room temperature naphtha is measured using a quart jar, then funneled into each jug. The height of the naphtha in the jug is mentally noted, so one can easily tell when all the emulsions and bubbles have settled out of the shaken mixture.

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Both jugs are shaken vigorously (one may want to not shake em so hard, but with this tek, separation still occurs fairly quickly, even when one shakes the beejesus out of them). These jugs were shaken vigorously several times, and placed in a heat bath, which consists of tap water in the plugged sink, as hot as it will go, and as high up on the jugs as possible, without overflowing the sink.

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After about 20 minutes, one can see the layers slowly starting to separate. This is why the mental note is taken when waiting for separation, as the layers are easy to see, but the emulsion layer is harder to see through the opaque jugs. One needs to wait, and the heat bath helps, until the layers are totally separated, before trying to remove the naphtha layer, or they will not get it all out very easily..

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In this case, after about 45 minutes or so, one can see they have separated nicely, and both layers are easily seen.

SWIM now takes a gatorade bottle, with the twist close type nozzle, and cuts the very bottom off of it. The bottle is rinsed out and the jugs of naphtha are slowly poured into the bottle, making sure the nozzle is twisted closed. By pouring slowly, one can manage to get very little MHRB sludge/water into the makeshift funnel.

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Here one can see that a little bit of the MHRB/lye water solution has gotten into the funnel, along with the majority of the solvent. Leaving about an 1/8 inch or so of solvent isn't a big worry, because when doing 3-4 pulls, there will be very little DMT left in that tiny, thin layer.

The makeshift funnel is then held over the open jug, and the twist nozzle is opened slowly, to allow the majority of MHRB juice to drain back into the original jug. Sometimes the hole can clog a bit with bark particles, but the solvent can still be easily poured off the top of the flexible make shift funnel if this happens. The solvent is collected in a fresh jug for washing later.

If one pours the solvent off of the top of the makeshift funnel, slowly, they can watch the little bit of leftover MHRB juice go down the ridges of the makeshift funnel, and they can be sure not to get any of that into the solvent collecting jug.

It's better to just pour a fine layer of solvent back into the extraction jug, than to get the MHRB juice into the solvent collection jug, but if either happens, one will wash the solvent anyways, or will do more pulls on the extraction jug and can get the majority of solvent in the next pull.

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Here you see that both jugs have been separated and the solvent layer from each combined into the collection jug. As stated, one can notice a fine layer of naphtha still floating on the MHRB juice, but more naphtha will be added for the next pull.

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SWIM used fresh naphtha for his first pull, but for the 2nd, 3rd, and 4th pulls, he uses naphtha that he had left from his last extraction. The DMT had been freeze precipitated out, and the used solvent was saved for the next extraction.

Here one can see that SWIM has added 400 mls more of the used solvent to each jug for beginning the second pull.

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Both jugs again were shaken vigorously, then placed back into the heat bath, with fresh hot water added in the heat bath, and left for another 20 minutes or so to separate..

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After about 20-30 minutes, one can again see the separation occurring in the jugs. Again, SWIM separates the solvent, using the makeshift separatory funnel made from the gatorade bottle. The solvent is collected into the collection jug again.

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Here is the second pull separated and, once again, you will notice that there is still a small layer of naphtha floating on the MHRB juice. Again, not to worry, the 3rd and fourth pulls will be done, and on the 4th, extra care will be used to try and get the majority. However, an 1/8 inch of solvent, with very little DMT in it, is usually not worth the bother..

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Here you will see another 400 mls of naphtha (again recycled from the previous extraction) added to both jugs, which are again shaken and placed into a heat bath.

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Fresh water is again run to keep the heat bath hot, and to allow faster separation. This was the third pull, but separation took extra long in one of the jugs, and since it was getting late, he didn't wait for total separation, because he was in a hurry. However, one can add more lye if this happens, or they can just let it continue to sit in a heat bath until full separation occurs.

So, a fourth pull was added to the jug, after he got off the majority of solvent that he could from both jugs. He again shook them vigorously (which may have been the reason the one jug took so long to separate), then placed them in the heat bath and separated, as shown in the previous 3 pulls. SWIm will leave the fourth pull and separation out of the pictorial, since the photos above show the process easily. The next pic shows after all 4 pulls have been done and separated..

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This shows what the jugs looked like after 4 pulls were done, and the solvent collected into the single collection jug. Again, you'll notice the one jug still having a bit of extra solvent that hasn't totally separated, and why it was good to take a mental note. SWIM decided that he was tired, and set the solvent jug in a heat bath, so DMT would not begin to precipitate out, and he set the two jugs back in as well, and called it a night.

The rest of the solvent that was taking long to separate out of the difficult jug, had finally separated out by morning, and so he removed the majority of it and added it to the solvent jug. This solvent was now ready to be washed and dried, then freeze precipitated.

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Here you'll see, he has gathered his sodium carbonate (pH Plus) and his epsom salts, along with his jug of DMT filled solvent. He gets a jar for mixing the sodium carbonate and water, takes his makeshift sep funnel, his 2 liter funnel, and another gallon jug, and places them all into his work area.

One trick to the polar wash, is doing it all fairly quickly. By not allowing the water to sit in the solvent for long after it separates (which happens in seconds), it makes sure that DMT is not ionized and pulled back into the water. Sodium carbonate also raises the PH of the water to above 9, where the DMT also will not ionize quickly, if at all.

In a pinch, sodium bicarbonate could be used, but should also been done very quickly, so as not to lose yields, since it doesn't raise the pH as high as the carbonate does.

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Here SWIM pours a thin layer of sodium carbonate into the jar. He then runs hot tap water into the jar and looks at the bottom of the jar, sometimes giving it a good stir, to just dissolve all the sodium carbonate.

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The wash water will look cloudy after first being mixed, but if left to settle for a few minutes, it will get clearer, and one can try to add a bit more sodium carbonate, to make sure it is saturated. If one can test the pH, just be sure that the pH of the water is 9 or 10 at least.

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Here one can see that SWIM has poured a small amount of the sodium carbonate water into the sep funnel.

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The sodium carbonate water is then drained into the solvent jug and shaken vigorously. The separation occurs within seconds.

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When the separation occurs, one will see the dark orange water layer. This is your polar impurities that were left in your solvent. Looks pretty nasty, right? That's why we want to do this wash, to pull out some of that color, and any residual lye.

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The majority of the solvent is poured from one jug, into a new jug.

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When the majority is poured off, one can see the water layer getting close to the nozzle. This mixture is then poured into the makeshift gatorade sep funnel.

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Another photo to show the separation closer..

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Here you'll see the mix poured into the sep funnel, and the bottom wash water layer is drained out, and the remaining solvent added back to the jug.

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The second wash is performed in the same way. The sodium carbonate water is placed into the funnel again.

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Here you can see it again being drained into the solvent jug.

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The jug has been shaken vigorously again and has settled. It is hard to see the tiny water layer in this pic, especially with the opaque jug, but if you look closely, you may be able to see it..

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Again, the majority of solvent is poured off the top, back into the other jug.

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SWIM has stopped pouring when he sees the water layer getting close, then transfers the mix back into his sep funnel. You see that all the color has been removed, and the water is clear.

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Here you can see the separation clearer, and how the wash water is much cleaner than in the first wash.

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Now, SWIM takes a tiny bit of cold tap water (pictured here) to do one more final wash. This one is the one that should be done quickly, because the PH of the water has not been adjusted with anything. SWIM's tap water comes out to a pH of about 7.5-8, but if left to sit in the naphtha, could ionize DMT. This is why just a tiny amount is used for a large amount of solvent, and why it is done quickly. Also, if there had been any carbonate or lye left in the solvent, this plain water wash will collect that, raising the PH of the water, and lowering the PH of the solvent. This ensures there will be no residual lye or contaminants in the final DMT. One could test this final cold tap water wash before and after to see how much lye is removed..

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Here you see the cold tap water wash being drained into the solvent, for the final, plain, cold tap water wash.

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Again, this is shaken vigorously, and it separates within seconds, although one can barely see the water layer. The majority of solvent is again poured into the other jug, until a small amount of solvent and the water layer are left. This is again poured into the makeshift sep funnel, and separated as shown in each previous step.

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The water layer is discarded again, and the solvent returned to the solvent collection jug.

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Here you can see some everyday epsom salts, purchasable from any local grocery or drug store.

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A thin layer is poured onto a microwave safe plate.

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Here you can see it is spread thinly over the plate. This is placed into the microwave on 5-10 minute on high to cook all the moisture out of the espom salt.

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After cooking it, you can see it is very white and crispy, and is stuck to the plate. NOTICE the oven mitt, the plate will be extremely hot, so handle with care. The cooked epsom salts are chipped away from the plate with a butter knife, and care is used so one does not get burnt by the hot plate.

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Here you can see the epsom salt chipped away, and then SWIM uses his fist or something hard to grind the chunks to a bit more powdery, with some chunks, as well..

The powder and chunks are added to the jug. SWIM doesn't measure, but just adds a few pinchfuls to the solvent, then he shakes it vigorously, so all the moisture that was left in the jug is soaked up and so no water can be seen in the bottom of the jug. This is left to settle, which also happens within seconds..

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Here you can see the espom salts collected in the bottom of the jug and all the moisture has been soaked up.

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The 2 liter funnel is upturned into a fresh, dry, clean jug, and a coffee filter is placed inside, to catch any epsom salt that falls out when pouring it into the fresh clean jug..

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Here you can see the solvent has been poured through the filter slowly, and any epsom salt is caught in the coffee filter..

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Here is the jug, now washed and dried, in a fresh, dry, clean jug, which is now ready to be placed in the freezer for anywhere from 12-72 hours. By waiting longer, the DMT settles out much better, and does not float in the solvent. This helps when pouring the solvent off the crystals slowly, into another jug, to be saved for future extractions..

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Here one can see the DMT settling out of the solvent that has been in the freezer for about 18 hours or so..

http://mycotopia.net...ictorial-51.jpg


Here is a large photo taken after the majority of solvent is poured off into a jug for later use. The top is then cut off of the jug, to reveal the huge pile of slightly yellow DMT, with tiny bit of residual solvent.

http://mycotopia.net...ictorial-52.jpg

This is the DMT after the solvent has dried up and the DMT has been scraped out of the jug. This chunky DMT is now spread thinly onto a glass baking dish, and chopped up finely, then placed in front of a box fan to continue drying completely.

http://mycotopia.net...ictorial-53.jpg

Once the solvent smell is gone and the crystals are thoroughly dried, they were placed back on the scale to show the yield and results..


So there you have it folks, a complete step by step pictorial of a simple STB, plus polar wash, and epsom salt dry, that anyone should be able to complete easily. This is what SWIM did, precisely, and got 17.1 grams of slightly yellow DMT, that will be recrystallized in days to come.

He'll take pics of the recrystallization procedure as well, then add them to this thread when he gets around to it. Until then, you'll have to go by the text in other threads..

Hope this helps clear up any questions, and shows exactly how simple the extraction is. No need for any extensive chemistry knowledge, and everything is easily found in most any neighborhood.

Use it wisely, and stay safe people!! Don't forget to share your DMT experiences and revelations here at Mycotopia, the best forum on the internet!!

:thumbup:

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Edited by wharfrat, 19 June 2016 - 04:02 PM.
fixed the photos

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#2 Om shanti

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Posted 05 September 2009 - 02:04 PM

Awesome stuff, thanks!
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#3 eastwood

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Posted 05 September 2009 - 02:13 PM

17g Wow! Great tek whatcha.Thanks for taking the time to put this thread together.Im looking forward to seeing how swim goes about recrystallizing the spice. :bow:

#4 whatchamacallit

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Posted 05 September 2009 - 02:17 PM

Mods, I accidentally uploaded number 14 pic first, and was wondering if it could be moved to the correct spot in the thumbnails part? If so, I'd appreciate it, and this post could be deleted, if not, just delete this post, and people can see it in order in the thread. The pics are also numbered 1-53, so they are labeled to go in order easily. If anyone would like to make this into a pdf file, feel free.
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#5 real_psily

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Posted 05 September 2009 - 03:22 PM

Damn Watcha that is 3.7+% yield!!
:bow::bow:
I can't tell how yellow that spice is by the pic, but looks good.
I'm sure it will look like glass when re-xtalized.

#6 whatchamacallit

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Posted 05 September 2009 - 05:27 PM

Damn Watcha that is 3.7+% yield!!
:bow::bow:
I can't tell how yellow that spice is by the pic, but looks good.
I'm sure it will look like glass when re-xtalized.

Not 3.7%. That was 908 grams of bark, give or take... He would have done the whole kilo, but figured since he only had two bottles of lye, he should just do it pound for pound.. The yield was 17.1 grams. So it would technically be 1.8832599118942731277533039647577 % (1.9%)

But we'll settle for probably a little over a half ounce of clear/white crystals, at least.. That is enough DMT to last for years. SWIM can play around a bit recrystallizing, maybe even a few times, as slow as possible, to get some really pretty, large, clear crystals and keep the concentrated yellow/orange stuff to get hard and crystallize, as well..
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#7 Raziel

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Posted 05 September 2009 - 06:02 PM

So friggen jealous :lol: Nice picterial whatchamacallit :bow:

#8 Shroomette

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Posted 05 September 2009 - 06:09 PM

You are all set now Whatcha.. I fixed all the photos.. Very excellent write up and great pictorial too thanks for sharing it hun :bow::heart:

#9 whatchamacallit

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Posted 05 September 2009 - 06:15 PM

You are all set now Whatcha.. I fixed all the photos.. Very excellent write up and great pictorial too thanks for sharing it hun :bow::heart:

Actually you moved them around in the post but did nothing to the thumbnail. They are now out of order with the captions but I'll fix it..

EDIT: Okay, thanks for the help ette, and now I replaced the pics into the right spots..

#10 Shroomette

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Posted 05 September 2009 - 06:24 PM

Actually you moved them around in the post but did nothing to the thumbnail. They are now out of order with the captions but I'll fix it..

UGH so sorry whatchamacallit... the dyslexia strikes again. But, at least they are tagged for ya hun.:heart: atleast it was just number 14 out of place.

#11 whatchamacallit

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Posted 05 September 2009 - 07:42 PM

Now they are back in order, but for some reason are shrinking!!! Oh well, they have all been deleted from my computer, so if they disappear, it's the end of this tek... Hope it gets sorted out... Hate to lose it all after all that work..


EDIT: I fixed it, there was a small letter t added in the links that made them the size of the thumbnail, but now they are the correct size. Number 31 I must have bumped a wrong button when i was resizing, but I didn't feel like trying to mess with it. Doesn't really make much difference, and is still able to be seen clearly enough.

#12 Raziel

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Posted 05 September 2009 - 08:17 PM

UGH so sorry whatchamacallit... the dyslexia strikes again. But, at least they are tagged for ya hun.:heart: atleast it was just number 14 out of place.


It was the thought that counts and it definatly there. Nice write up (again)

#13 real_psily

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Posted 05 September 2009 - 08:31 PM

Not 3.7%. That was 908 grams of bark, give or take...

LMFAO
read too quick and saw 454
I see you did that x2
Still nice work:bow::bow:

#14 buteo

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Posted 05 September 2009 - 09:32 PM

good work whatcha ....thank you for this !

#15 whatchamacallit

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Posted 05 September 2009 - 09:44 PM

http://mycotopia.net...=1&d=1252204909


Here is number 31 in the proper size, but it's too late for me to add it to the post. However, if anyone can make this into a pdf file with the captions and photos in the right place, here is number 31, done to about the same size as the other photos, in the thread, so this one could be exchanged for the number 31 in the original post.

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#16 LotRev

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Posted 06 September 2009 - 05:52 AM

Bad-Fucking-Ass my friend.

Nice pictorial...so we don't need anymore DMT discussion eh,
you've got it all covered now? :lol:

Really, excellent job Whatcha, thank you for posting this.
I bet it starts popping up all over the place.

:eusa_clap

#17 eatyualive

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Posted 06 September 2009 - 12:48 PM

wow very nice. im gonna have to give this another go.

#18 Shadowlord

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Posted 06 September 2009 - 12:56 PM

wow very nice. im gonna have to give this another go.



If you had less than great results b4 then definitely try again Eats.
I had more trouble working w/ DMT than I did mescaline at frist, but after you have run the MHRB extraction a few times you just get the knack for it and it all starts to work for you.
I still don't smoke DMT often but it is amazing stuff when the mood strikes.
Good luck Eats and to anyone else contemplating extracting.

#19 Shadowlord

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Posted 06 September 2009 - 12:59 PM

And great thread BTW Whatcha.
Yours is what I envisioned mine to be a while back. But I just wasn't anywhere near as thorough.
Some fine work. I'm sure we'll be seeing your work pop up all over the place.
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#20 LotRev

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Posted 06 September 2009 - 03:46 PM

Hey Whatcha, I did just a tad of clean up and formatting and made this thing into a pdf.
The file is attached for anyone to download and share.

ok, added a title, didn't know if you wanted your name on it

(this is the highest quality it can be done and uploaded here)

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